Chiral Nanochannels of Ordered Mesoporous Silica Constructed by a Pillar[5]arene-Based Host-Guest System

ACS Appl Mater Interfaces. 2021 Jun 16;13(23):27305-27312. doi: 10.1021/acsami.1c05790. Epub 2021 Jun 2.

Abstract

The separation of racemic compounds by chiral nanochannels has attracted extensive attention. However, the fabrication of high-performance chiral nanochannels is still a challenge owing to the difficulty in magnifying the weak chiral interaction to macroscopic properties of materials. Herein, by introducing a l-alanine-pillar[5]arene host to achiral ordered mesoporous silica (OMS), chiral OMS nanochannels were fabricated, which exhibited excellent selectivity (ee value up to 90.2%) to separate racemic drugs with promising reusability and stability. Besides, it was identified that enantioselective separation took place through a molecular-recognition-adsorbed transport mechanism. This work highlights the great potential of chiral OMS nanochannels as a platform for enantioselective separation.

Keywords: chiral nanochannel; chiral resolution; host−guest system; membrane separation; ordered mesoporous silica.