Formulation and Evaluation of Baclofen-Meloxicam Orally Disintegrating Tablets (ODTs) Using Co-Processed Excipients and Improvement of ODTs Performance Using Six Sigma Method

Drug Des Devel Ther. 2021 Oct 16:15:4383-4402. doi: 10.2147/DDDT.S327193. eCollection 2021.

Abstract

Purpose: This study aimed to formulate an orally disintegrating tablet (ODT) containing both baclofen and meloxicam together for treating osteoarthritis.

Methods: Direct compression method was used to prepare ODTs using three types of co-processed excipients (Prosolv ODT G2®, F-melt®, and Pharmaburst®500). ODTs were evaluated according to weight variation, thickness, friability, hardness, drug content, wetting time, in-vitro disintegration time, in-vitro dissolution test, and palatability. To enhance the in-vitro dissolution of meloxicam and palatability of ODT, a six sigma methodology was used, and an improvement phase was established where ODTs were prepared using lyophilization and levigation techniques. Finally, a pharmacokinetic study of the improved ODT was accomplished in comparison to the conventional oral tablet.

Results: Pharmaburst-based formula (F4) showed the shortest wetting time and, consequently, the shortest disintegration time and the highest percentage of drug dissolved within 3 min compared to the other formulae. All the improved ODTs had a bitterness taste score vary from (0) palatable and (+1) tasteless. The current sigma level was 3.628 σ and 3.33 σ for palatability and solubility of ODT, respectively, which indicated the process was successfully improved compared with the previous sigma level of 2.342 σ of both processes. Pharmacokinetic study of the improved ODTs showed a significant decrease of Tmax to 120 and 30 min instead of 180 and 120 min for meloxicam and baclofen, respectively.

Conclusion: ODTs were successfully improved using the six sigma methodology, the pharmacokinetic parameters of both drugs were enhanced due to rapid absorption through the oral mucosa.

Keywords: baclofen; co-processed excipients; meloxicam; orally disintegrating tablet; six sigma methodology.

Publication types

  • Comparative Study

MeSH terms

  • Administration, Oral
  • Adult
  • Baclofen / administration & dosage*
  • Baclofen / chemistry
  • Baclofen / pharmacokinetics
  • Drug Compounding
  • Drug Liberation
  • Excipients / chemistry*
  • Female
  • Freeze Drying
  • Humans
  • Male
  • Meloxicam / administration & dosage*
  • Meloxicam / chemistry
  • Meloxicam / pharmacokinetics
  • Muscle Relaxants, Central / administration & dosage*
  • Muscle Relaxants, Central / chemistry
  • Muscle Relaxants, Central / pharmacokinetics
  • Solubility
  • Tablets
  • Taste
  • Total Quality Management

Substances

  • Excipients
  • Muscle Relaxants, Central
  • Tablets
  • Baclofen
  • Meloxicam