Novel dual-functional implants via oxygen non-thermal plasma and quaternary ammonium to promote osteogenesis and combat infections

Dent Mater. 2022 Jan;38(1):169-182. doi: 10.1016/j.dental.2021.12.001. Epub 2021 Dec 16.

Abstract

Objective: Implant-related infections are a primary reason for implant failures that affect millions of patients. It is of paramount importance to develop novel implants that possess the dual functions of osteogenesis-promotion and antibacterial activity. The objectives of this study were to: (1) develop novel dual-functional titanium (Ti) implants by combining oxygen non-thermal plasma and covalent bonding of antibacterial organosilicon quaternary ammonium monomers; (2) investigate the physicochemical properties, bioactivity and antibacterial effects of the modified implants for the first time.

Methods: Surface characteristics of the modified Ti surfaces were tested. Adherence and viability of rat bone marrow-derived stem cells (rBMSCs) on the surface were evaluated. Metabolic activity of biofilm on the surfaces were measured. The stability of the dual-function after 5000 thermal cycles was also evaluated.

Results: The presence of chemical bonding between Ti and organosilicon monomers demonstrated covalent immobilization of the antibacterial agents. The water contact angle of the treated Ti surfaces decreased from 70.98 ± 3.68° to 59.86 ± 4.91°. The adhesion and proliferation of rBMSCs on the modified Ti were increased by 40%, compared to control group (P < 0.05). The metabolic level of biofilms on modified Ti were reduced by more than half, compared to control (P < 0.05). The modified Ti implants exhibited cell-promotion and antibacterial stability after thermal cycles.

Significance: The new dual-functional Ti implant is promising to promote osteogenesis while simultaneously preventing infections. Furthermore, the novel surface modification and processing methods have applicability to enhancing a wide range of other implants to improve bioactivity and combat infections.

Keywords: Antibacterial; Implant-related infections; Non-thermal plasma; Organosilicon quaternary ammonium; Osteogenesis; Stem cells.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Ammonium Compounds* / pharmacology
  • Animals
  • Anti-Bacterial Agents / chemistry
  • Anti-Bacterial Agents / pharmacology
  • Dental Implants*
  • Humans
  • Osteogenesis
  • Oxygen
  • Rats
  • Surface Properties
  • Titanium / chemistry
  • Titanium / pharmacology

Substances

  • Ammonium Compounds
  • Anti-Bacterial Agents
  • Dental Implants
  • Titanium
  • Oxygen