Calcium ion cross-linked sodium alginate hydrogels containing deferoxamine and copper nanoparticles for diabetic wound healing

Int J Biol Macromol. 2022 Mar 31:202:657-670. doi: 10.1016/j.ijbiomac.2022.01.080. Epub 2022 Jan 20.

Abstract

Chronic non-healing diabetic wounds and ulcers can be fatal, lead to amputations, and remain a major challenge to medical, and health care sectors. Susceptibility to infection and impaired angiogenesis are two central reasons for the clinical consequences associated with chronic non-healing diabetic wounds. Herein, we successfully developed calcium ion (Ca2+) cross-linked sodium alginate (SA) hydrogels with both pro-angiogenesis and antibacterial properties. Our results demonstrated that deferoxamine (DFO) and copper nanoparticles (Cu-NPs) worked synergistically to enhance the proliferation, migration, and angiogenesis of human umbilical venous endothelial cells in vitro. Results of colony formation assay indicated Cu-NPs were effective against E. coli and S. aureus in a dose-dependent manner in vitro. An SA hydrogel containing both DFO and Cu-NPs (SA-DFO/Cu) was prepared using a Ca2+ cross-linking method. Cytotoxicity assay and colony formation assay indicated that the hydrogel exhibited beneficial biocompatible and antibacterial properties in vitro. Furthermore, SA-DFO/Cu significantly accelerated diabetic wound healing, improved angiogenesis and reduced long-lasting inflammation in a mouse model of diabetic wound. Mechanistically, DFO and Cu-NPs synergistically stimulated the levels of hypoxia-inducible factor 1α and vascular endothelial growth factor in vivo. Given the pro-angiogenesis, antibacterial and healing properties, the hydrogel possesses high potential for clinical application in refractory wounds.

Keywords: Copper nanoparticles; Deferoxamine; Diabetic wound; Hydrogel.

MeSH terms

  • Alginates
  • Animals
  • Calcium
  • Copper
  • Deferoxamine / pharmacology
  • Diabetes Mellitus*
  • Escherichia coli
  • Human Umbilical Vein Endothelial Cells
  • Humans
  • Hydrogels / pharmacology
  • Mice
  • Nanoparticles*
  • Staphylococcus aureus
  • Vascular Endothelial Growth Factor A
  • Wound Healing

Substances

  • Alginates
  • Hydrogels
  • Vascular Endothelial Growth Factor A
  • Copper
  • Deferoxamine
  • Calcium