Insights in the Synthesis of Imidazolones from Aldehydes, Isocyanides, or Oxazolines

J Org Chem. 2022 Jun 3;87(11):7464-7473. doi: 10.1021/acs.joc.1c02454. Epub 2022 May 15.

Abstract

α-Isocyanoacetamide derivatives were first converted to oxazolines under newly developed conditions. These oxazolines were used as precursors of α-isocyanoacrylamides, which could lead to various 2-arylated imidazolones. In addition, it was shown that both oxazolines and their precursors could efficiently lead to imidazolones unsubstituted at C2 in a very rapid, one-pot transformation, thus paving the way toward unprecedented routes to imidazolones, having a good tolerance to different substitution patterns.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aldehydes*
  • Cyanides*
  • Imidazoles

Substances

  • Aldehydes
  • Cyanides
  • Imidazoles
  • imidazolone