Palladium-catalyzed stereoselective ring-opening reaction of aryl cyclopropyl ketones

Org Biomol Chem. 2022 Jul 13;20(27):5412-5415. doi: 10.1039/d2ob00719c.

Abstract

Herein, we report that α,β-unsaturated ketones could be obtained by palladium-catalyzed ring-opening of mono-substituted cyclopropyl ketones efficiently and systematically. (E)-1-Arylbut-2-en-1-ones were generated from aryl cyclopropyl ketones stereoselectively in yields of 23-89% by the Pd(OAc)2/PCy3 catalytic system. The reaction exhibited stereoselectivity (only E products were found) and was suitable for both phenyl and heteroaryl cyclopropyl ketones.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Catalysis
  • Ketones*
  • Molecular Structure
  • Palladium*

Substances

  • Ketones
  • Palladium