Wiring of bilirubin oxidases with redox polymers on gas diffusion electrodes for increased stability of self-powered biofuel cells-based glucose sensing

Bioelectrochemistry. 2023 Feb:149:108314. doi: 10.1016/j.bioelechem.2022.108314. Epub 2022 Oct 27.

Abstract

A new redox polymer/bilirubin oxidase (BOD)-based gas diffusion electrode was designed to be implemented as the non-current and non-stability limiting biocathode in a glucose/O2 biofuel cell that acts as a self-powered glucose biosensor. For the proof-of-concept, a bioanode comprising the Os-complex modified redox polymer P(VI-co-AA)-[Os(bpy)2Cl]Cl and FAD-dependent glucose dehydrogenase to oxidize the analyte was used. In order to develop an optimal O2-reducing biocathode for the biofuel cell Mv-BOD as well as Bp-BOD and Mo-BOD have been tested in gas diffusion electrodes in direct electron transfer as well as in mediated electron transfer immobilized in the Os-complex modified redox polymer P(VI-co-AA)-[Os(diCl-bpy)2]Cl2. The resulting biofuel cell exhibits a glucose-dependent current and power output in the concentration region between 1 and 10 mM. To create a more realistic test environment, the performance and long-term stability of the biofuel cell-based self-powered glucose biosensor has been investigated in a flow-through cell design.

Keywords: Bilirubin oxidase; Gas diffusion electrode; Glucose sensor; Oxygen reduction; Redox polymer.

MeSH terms

  • Bilirubin
  • Bioelectric Energy Sources*
  • Biosensing Techniques*
  • Electrodes
  • Enzymes, Immobilized / metabolism
  • Gases
  • Glucose
  • Glucose 1-Dehydrogenase / metabolism
  • Oxidation-Reduction
  • Oxidoreductases Acting on CH-CH Group Donors* / metabolism
  • Polymers

Substances

  • Bilirubin
  • bilirubin oxidase
  • Enzymes, Immobilized
  • Glucose
  • Glucose 1-Dehydrogenase
  • Oxidoreductases Acting on CH-CH Group Donors
  • Polymers
  • Gases