Independent Membrane Binding Properties of the Caspase Generated Fragments of the Beaded Filament Structural Protein 1 (BFSP1) Involves an Amphipathic Helix

Cells. 2023 Jun 7;12(12):1580. doi: 10.3390/cells12121580.

Abstract

Background: BFSP1 (beaded filament structural protein 1) is a plasma membrane, Aquaporin 0 (AQP0/MIP)-associated intermediate filament protein expressed in the eye lens. BFSP1 is myristoylated, a post-translation modification that requires caspase cleavage at D433. Bioinformatic analyses suggested that the sequences 434-452 were α-helical and amphipathic.

Methods and results: By CD spectroscopy, we show that the addition of trifluoroethanol induced a switch from an intrinsically disordered to a more α-helical conformation for the residues 434-467. Recombinantly produced BFSP1 fragments containing this amphipathic helix bind to lens lipid bilayers as determined by surface plasmon resonance (SPR). Lastly, we demonstrate by transient transfection of non-lens MCF7 cells that these same BFSP1 C-terminal sequences localise to plasma membranes and to cytoplasmic vesicles. These can be co-labelled with the vital dye, lysotracker, but other cell compartments, such as the nuclear and mitochondrial membranes, were negative. The N-terminal myristoylation of the amphipathic helix appeared not to change either the lipid affinity or membrane localisation of the BFSP1 polypeptides or fragments we assessed by SPR and transient transfection, but it did appear to enhance its helical content.

Conclusions: These data support the conclusion that C-terminal sequences of human BFSP1 distal to the caspase site at G433 have independent membrane binding properties via an adjacent amphipathic helix.

Keywords: amphipathic helix; cataract; intermediate filaments; intrinsically disordered domain; lens; lipid binding; membrane scaffold; oligomerisation; post-translational myristoylation.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Caspases* / metabolism
  • Cell Membrane / metabolism
  • Humans
  • Intermediate Filament Proteins / metabolism
  • Lens, Crystalline* / metabolism
  • Membranes / metabolism

Substances

  • Caspases
  • Intermediate Filament Proteins
  • filensin

Grants and funding

This work was supported by funding from Fight for Sight (M.J., A.T., R.A.Q.; Fight for Sight UK grant #1584/85) and from the National Eye Research Charity (A.K.K.; SAC014) are gratefully acknowledged. AW was funded via the LDLensRad project that received funding from the Euratom research and training programme 2014–2018 in the framework of the CONCERT (grant agreement No. 662287). E.N.W. and K.L. were funded by a vacation scholarship from the Biophysical Sciences Institute. This publication reflects only the author’s view. Responsibility for the information and views expressed therein lies entirely with the authors. The European Commission is not responsible for any use that may be made of the information it contains.