A Building Block Approach for the Total Synthesis of YM-385781

European J Org Chem. 2023 May 22;26(20):e202300365. doi: 10.1002/ejoc.202300365. Epub 2023 Apr 25.

Abstract

YM-254890 and FR900359 are potent and selective inhibitors of the Gq/11-signaling pathway. As such, they have been attractive targets for both synthesis and biological studies. Yet in spite of this effort, a versatile synthetic approach to the molecules that allows for the rapid construction of a variety of non-natural and labelled analogs and an increase in the amount of those analogs available remains elusive. We report here a convergent building block approach to the molecules that can solve this challenge.

Keywords: Cyclic Peptide Synthesis; Inhibitors; YM-analogs.