Thermoresponsive Core-cross-linked Nanoparticles from HA- b-ELP Diblock Copolymers

Biomacromolecules. 2024 May 13;25(5):3011-3017. doi: 10.1021/acs.biomac.4c00137. Epub 2024 Apr 30.

Abstract

Stabilization against the dilution-dependent disassembly of self-assembled nanoparticles is a requirement for in vivo application. Herein, we propose a simple and biocompatible cross-linking reaction for the stabilization of a series of nanoparticles formed by the self-assembly of amphiphilic HA-b-ELP block copolymers, through the alkylation of methionine residues from the ELP block with diglycidyl ether compounds. The core-cross-linked nanoparticles retain their colloidal properties, with a spherical core-shell morphology, while maintaining thermoresponsive behavior. As such, instead of a reversible disassembly when non-cross-linked, a reversible swelling of nanoparticles' core and increase of hydrodynamic diameter are observed with lowering of the temperature.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cross-Linking Reagents* / chemistry
  • Elastin / chemistry
  • Nanoparticles* / chemistry
  • Particle Size
  • Polymers / chemistry
  • Temperature

Substances

  • Cross-Linking Reagents
  • Polymers
  • Elastin