Enantioselective Syntheses of 3,4-Dihydropyrans Employing Isochalcogenourea-Catalyzed Formal (4+2)-Cycloadditions of Allenoates

Adv Synth Catal. 2024 May 21;366(9):2115-2122. doi: 10.1002/adsc.202400038. Epub 2024 Mar 4.

Abstract

We herein successfully demonstrate the use of chiral isochalcogenoureas as Lewis Base catalysts for a variety of (4+2)-cycloaddition reactions of allenoates and different Michael acceptors. In all cases the same structural key-motive, a dihydropyran with a (Z)-configurated exocyclic double bond could be accessed as the major regio- and diastereoisomer in an enantioselective manner. Furthermore, these chiral dihydropyrans were successfully engaged in different follow-up transformations.

Keywords: Allenoates; Cycloadditions; Isochal-cogenoureas; Lewis Bases; Organocatalysis.