Catalytic Enantioselective Sulfoxidation of Functionalized Thioethers Mediated by Aspartic Acid-Containing Peptides

Org Lett. 2024 Aug 16;26(32):6872-6877. doi: 10.1021/acs.orglett.4c02452. Epub 2024 Aug 5.

Abstract

A peptide-catalyzed enantioselective oxidation of sulfides to yield pharmaceutically relevant chiral sulfoxides is reported. Experimental evidence suggesting that a hydrogen bond-donating moiety must be present in the substrate to achieve high levels of enantioinduction is supported by computational modeling of transition states. These models also indicate that dual points of contact between the peptidic catalyst and substrate are likely responsible for the formation of one desired sulfoxide in 94:6 er.

MeSH terms

  • Aspartic Acid* / chemistry
  • Catalysis
  • Hydrogen Bonding
  • Molecular Structure
  • Oxidation-Reduction*
  • Peptides* / chemical synthesis
  • Peptides* / chemistry
  • Stereoisomerism
  • Sulfides* / chemistry
  • Sulfoxides* / chemistry

Substances

  • Peptides
  • Sulfides
  • Aspartic Acid
  • Sulfoxides