The activity of therapeutic molecular cluster Ag5 is dependent on oxygen level and HIF-1 mediated signalling

Redox Biol. 2024 Oct:76:103326. doi: 10.1016/j.redox.2024.103326. Epub 2024 Aug 22.

Abstract

Regions of hypoxia occur in most solid tumours and are known to significantly impact therapy response and patient prognosis. Ag5 is a recently reported silver molecular cluster which inhibits both glutathione and thioredoxin signalling therefore limiting cellular antioxidant capacity. Ag5 treatment significantly reduces cell viability in a range of cancer cell lines with little to no impact on non-transformed cells. Characterisation of redox homeostasis in hypoxia demonstrated an increase in reactive oxygen species and glutathione albeit with different kinetics. Significant Ag5-mediated loss of viability was observed in a range of hypoxic conditions which mimic the tumour microenvironment however, this effect was reduced compared to normoxic conditions. Reduced sensitivity to Ag5 in hypoxia was attributed to HIF-1 mediated signalling to reduce PDH via PDK1/3 activity and changes in mitochondrial oxygen availability. Importantly, the addition of Ag5 significantly increased radiation-induced cell death in hypoxic conditions associated with radioresistance. Together, these data demonstrate Ag5 is a potent and cancer specific agent which could be used effectively in combination with radiotherapy.

Keywords: Ag5; HIF-1; Hypoxia; Radiation; Redox.

MeSH terms

  • Antineoplastic Agents / pharmacology
  • Cell Hypoxia
  • Cell Line, Tumor
  • Cell Survival* / drug effects
  • Glutathione / metabolism
  • Humans
  • Hypoxia-Inducible Factor 1 / metabolism
  • Hypoxia-Inducible Factor 1, alpha Subunit / metabolism
  • Mitochondria / drug effects
  • Mitochondria / metabolism
  • Neoplasms / drug therapy
  • Neoplasms / metabolism
  • Neoplasms / pathology
  • Oxidation-Reduction
  • Oxygen* / metabolism
  • Protein Serine-Threonine Kinases / metabolism
  • Pyruvate Dehydrogenase Acetyl-Transferring Kinase / metabolism
  • Reactive Oxygen Species* / metabolism
  • Signal Transduction* / drug effects
  • Silver / chemistry

Substances

  • Oxygen
  • Reactive Oxygen Species
  • Glutathione
  • Hypoxia-Inducible Factor 1, alpha Subunit
  • PDK1 protein, human
  • Pyruvate Dehydrogenase Acetyl-Transferring Kinase
  • Protein Serine-Threonine Kinases
  • HIF1A protein, human
  • Hypoxia-Inducible Factor 1
  • Silver
  • Antineoplastic Agents