Silver-Catalyzed Carbamoylation and Carbonylative Cyclization of Alkenes with Oxamic Acids

Chem Asian J. 2024 Dec 2;19(23):e202400892. doi: 10.1002/asia.202400892. Epub 2024 Oct 23.

Abstract

Transition metal-catalyzed carbonylation functionalization reaction of alkenes is an attractive research area in modern organic chemistry. However, there have been very few reports on silver-catalyzed reactions in carbonylation reactions. Herein we developed a silver-catalyzed carbamoylation and carbonylative cyclization of alkenes with oxamic acids to obtain 2-acetylamino-1-tetralone derivatives. Various desired cyclized products were formed in moderate to good yields through radical intermediates.

Keywords: carbonylation; cyclization; radical; silver catalyst; tetralone.