Engineered PLGA Core-Lipid Shell Hybrid Nanocarriers Improve the Efficacy and Safety of Irinotecan to Combat Colon Cancer

ACS Biomater Sci Eng. 2024 Oct 14;10(10):6661-6676. doi: 10.1021/acsbiomaterials.4c01260. Epub 2024 Sep 13.

Abstract

Poly(lactide-co-glycolide) (PLGA) is a biocompatible and biodegradable copolymer that has gained high acceptance in biomedical applications. In the present study, PLGA (Mw = 13,900) was synthesized by ring-opening polymerization in the presence of a biocompatible zinc-proline initiator through a green route. Irinotecan (Ir) loaded with efficient PLGA core-lipid shell hybrid nanocarriers (lipomers, LPs) were formulated with 1,2-distearoyl-sn-glycero-3-phosphoethanolamine and 1,2-distearoyl-sn-glycero-3-phosphoethanolamine-N-[amino (polyethylene glycol)-2000] (DSPE-PEG-2000), using soya lecithin, by a nanoprecipitation method, and the fabricated LPs were designated as P-DSPE-Ir and P-DSPE-PEG-Ir, respectively. The formulated LPs were further validated for their physicochemical properties and biological potential for colon cancer application. The potential delivery of a poorly water-soluble chemotherapeutic drug (Ir) was studied for the treatment of colon cancer. LPs were successfully prepared, providing controlled size (80-120 nm) and surface charge (∼ -35 mV), and the sustained release properties and cytotoxicity against CT-26 colon cancer cells were studied. The in vivo biodistribution and tumor site retention in CT-26 xenograft tumor-bearing Balb/C mice showed promising results for tumor uptake and retention for a prolonged time period. Unlike P-DSPE-Ir, the P-DSPE-PEG-Ir LP exhibited significant tumor growth delay as compared to untreated and blank formulation-treated groups in CT-26 (subcutaneous tumor model) after 4 treatments of 10 mg irinotecan/kg dose. The biocompatibility and safety of the LPs were confirmed by an acute toxicity study of the optimized formulation. Overall, this proof-of-concept study demonstrates that the PLGA-based LPs improve the efficacy and bioavailability and decrease neutropenia of Ir to combat colon cancer.

Keywords: CT-26; PLGA; chemotherapy; colon cancer; drug delivery; irinotecan; lipomer; neutropenia.

MeSH terms

  • Animals
  • Camptothecin / administration & dosage
  • Camptothecin / analogs & derivatives
  • Camptothecin / chemistry
  • Camptothecin / pharmacokinetics
  • Camptothecin / pharmacology
  • Camptothecin / therapeutic use
  • Cell Line, Tumor
  • Colonic Neoplasms* / drug therapy
  • Colonic Neoplasms* / pathology
  • Drug Carriers* / chemistry
  • Female
  • Humans
  • Irinotecan* / administration & dosage
  • Irinotecan* / chemistry
  • Irinotecan* / pharmacokinetics
  • Irinotecan* / pharmacology
  • Irinotecan* / therapeutic use
  • Lipids / chemistry
  • Mice
  • Mice, Inbred BALB C
  • Nanoparticles / chemistry
  • Nanoparticles / therapeutic use
  • Phosphatidylethanolamines / chemistry
  • Polyethylene Glycols* / chemistry
  • Polylactic Acid-Polyglycolic Acid Copolymer* / chemistry

Substances

  • Irinotecan
  • Drug Carriers
  • Polylactic Acid-Polyglycolic Acid Copolymer
  • Polyethylene Glycols
  • Phosphatidylethanolamines
  • polyethylene glycol-distearoylphosphatidylethanolamine
  • Camptothecin
  • Lipids