Synthesis and Characterization of β-Myrcene-Styrene and β-Ocimene-Styrene Copolymers

Macromol Rapid Commun. 2025 Jan;46(2):e2400641. doi: 10.1002/marc.202400641. Epub 2024 Oct 14.

Abstract

The structure-properties relationships of sustainable materials derived from biomass-based monomers are investigated, focusing on hybrid styrene/terpene-based copolymers with blocky microstructures, such as β-myrcene- and β-ocimene-styrene copolymers. The samples show complex glass transition dynamics, as evidenced by the physical aging experienced by the amorphous phase in styrene-rich copolymers. The tendency of styrene- and terpene-rich sequences to give heterogeneous morphologies with correlation strength extending over 10-40 nm is outlined, through small-angle X-ray scattering analysis. A new class of terpene-based hybrid systems, holding promise for applications in surface coating technologies, is identified.

Keywords: biomass polymers; biopolymers; circular economy polymers; renewable and biodegradable polymers; sustainable thermoplastics.

MeSH terms

  • Acyclic Monoterpenes* / chemistry
  • Alkanes / chemistry
  • Alkenes* / chemistry
  • Molecular Structure
  • Polymers* / chemical synthesis
  • Polymers* / chemistry
  • Polystyrenes / chemistry
  • Styrene / chemistry

Substances

  • Polymers
  • Alkenes
  • Acyclic Monoterpenes
  • beta-ocimene
  • myrcene
  • Styrene
  • Alkanes
  • Polystyrenes