Enhanced antitumor immunity in breast cancer: Synergistic effects of ADAM10/ADAM17 inhibition, metabolic modulation, and camptothecin-loaded selenium nanoparticles

Int J Pharm. 2025 Jan 25:669:125037. doi: 10.1016/j.ijpharm.2024.125037. Epub 2024 Dec 13.

Abstract

Background: In this study, we investigate the impact of a multi-targeted therapeutic approach that includes camptothecin (CPT), a potent chemotherapeutic topoisomerase inhibitor; metformin (Met), a metabolic modulator with emerging anti-tumor effects; and GW280264X, an inhibitor of ADAM 10/ADAM 17 enzymes, which are associated with tumor invasion and immune response. The study aims to assess the combined effects of these agents in enhancing CD8+ T cell-mediated anti-tumor immunity and suppressing cancer cell growth in triple-negative breast cancer (TNBC) models, both in vitro and in vivo.

Methods: Cell viability was performed on the 4 T1 human TNBC cell line. Furthermore, we examined c-MYC protein expression by western blot, TOX and NR4A expression by Real-time PCR, and the number of CD8+ CD28+ T cells by immunofluorescence assay to demonstrate the anticancer effects of combined of CPT, Met and GW280264X in BC growth, exhaustion and senescence of T cells.

Results: Regarding cell viability, HA-Se@CPT + Met and HA-Se@CPT + Met + GW280264X treatments decreased 4 T1 cell growth (p < 0.001). Combination therapy of Met, HA-Se@CPT, and GW280264X significantly reduced tumor volume and weight in vivo. This treatment also increased the number of CD8+ CD28+ T cells in the tumor microenvironment (TME) of BC (p < 0.0001) and decreased the expression of TOX and NR4A (p < 0.0001, p < 0.01). Furthermore, decreased expression of c-MYC as an oncogene protein was seen in the single and combined treatment by HA-Se@CPT and GW280264X (p < 0.05).

Conclusion: These findings suggest that of HA-Se@CPT, Met, and GW280264X may inhibit tumor progression in BC by improving the function and infiltration of CD8+ T cells. Their effect is more pronounced when used in combination.

Keywords: Breast cancer; CD8(+) T cell; Camptothecin; GW280264X; Metformin.

MeSH terms

  • Animals
  • CD8-Positive T-Lymphocytes* / drug effects
  • Camptothecin* / administration & dosage
  • Camptothecin* / analogs & derivatives
  • Camptothecin* / pharmacology
  • Cell Line, Tumor
  • Cell Survival* / drug effects
  • Drug Synergism
  • Female
  • Humans
  • Metformin* / administration & dosage
  • Metformin* / pharmacology
  • Mice
  • Mice, Inbred BALB C
  • Mice, Nude
  • Nanoparticles* / administration & dosage
  • Triple Negative Breast Neoplasms* / drug therapy
  • Triple Negative Breast Neoplasms* / immunology
  • Xenograft Model Antitumor Assays

Substances

  • Camptothecin
  • Metformin