Molten Metal Synthesis of Nanographenes

J Am Chem Soc. 2025 Jan 8;147(1):111-117. doi: 10.1021/jacs.4c16328. Epub 2024 Dec 23.

Abstract

This manuscript describes a simple and effective method to cyclodehydrogenate arenes using liquid alkali metals. Direct reaction between molten potassium and arenes forms 6-membered rings and zigzag edged structures within polyarenes. The approach is extended to integration of pyridinic nitrogen and 5-membered rings to arene structures and synthesis of larger, open-shell nanographenes.