Transient Directing Group-Assisted Palladium-Catalyzed C4-Alkynylation of Indoles

J Org Chem. 2025 Jan 10. doi: 10.1021/acs.joc.4c02478. Online ahead of print.

Abstract

Pd-catalyzed C4-selective alkynylation of indoles was established by employing glycine as a transient directing group. This reaction exhibits high regioselectivity with the tolerance of a wide scope of functional groups to afford diverse alkynylated indoles in moderate to good yields. Moreover, the readily accessible scale-up synthesis and further decorations to achieve multifunctionalized indoles demonstrate the synthetic potential of this protocol.