Delta-aminolevulinate increases heme saturation and yield of human cystathionine beta-synthase expressed in Escherichia coli

Arch Biochem Biophys. 1995 Jan 10;316(1):24-9. doi: 10.1006/abbi.1995.1005.

Abstract

We recently expressed human cystathionine beta-synthase (CBS) in Escherichia coli and purified it to homogeneity. We showed that CBS requires heme in addition to pyridoxal 5'-phosphate for its function. Previously, CBS, only about 20% saturated with heme, was purified from transformed bacteria. In the present study, we supplemented the bacteria with 0.3 mM delta-aminolevulinate (delta ALA), a precursor of heme. While growth of the bacteria did not change, a 50-fold elevation of the heme content per milligram of total protein was observed in the cell extracts of delta ALA-supplemented cells. The increase in heme biosynthesis depended on the overexpression of a heme acceptor--CBS. Our data suggest that bacterial heme synthesis is regulated beyond delta ALA synthase. The delta ALA treatment resulted in 8 times more total CBS activity with a 3.5-fold higher yield of the purified recombinant enzyme, more than 68% saturated with heme. Increased yield, higher specific activity, and improved heme saturation of CBS will facilitate large-scale preparation of the enzyme. This method should be applicable to the overexpression of other recombinant heme proteins in bacteria.

MeSH terms

  • Aminolevulinic Acid / pharmacology*
  • Cystathionine beta-Synthase / biosynthesis*
  • Cystathionine beta-Synthase / drug effects
  • Cystathionine beta-Synthase / genetics
  • Cystathionine beta-Synthase / isolation & purification
  • Escherichia coli / genetics
  • Escherichia coli / metabolism*
  • Heme / metabolism*
  • Hemeproteins / biosynthesis*
  • Hemeproteins / drug effects
  • Hemeproteins / genetics
  • Hemeproteins / isolation & purification
  • Humans
  • Recombinant Fusion Proteins / biosynthesis
  • Recombinant Fusion Proteins / drug effects
  • Spectrophotometry
  • beta-Galactosidase / biosynthesis
  • beta-Galactosidase / genetics

Substances

  • Hemeproteins
  • Recombinant Fusion Proteins
  • Heme
  • Aminolevulinic Acid
  • beta-Galactosidase
  • Cystathionine beta-Synthase