Labeling of basic fibroblast growth factor with digoxigenin: a nonradioactive probe for biochemical and cytological applications

Anal Biochem. 1994 Jun;219(2):360-7. doi: 10.1006/abio.1994.1277.

Abstract

Digoxigenin, a 391-Da plant sterol, was conjugated to recombinant bFGF with the aim of detecting it with high specificity and sensitivity in cultured eukaryotic cells using antibodies against digoxigenin. The conjugate, bFGF-DIG, displayed a mitogenic activity on endothelial cells equivalent to that of nonlabeled bFGF. Binding of the probe on the cell surface was assessed by ELISA on cells, which allowed discrimination between low- and high-affinity bFGF binding sites. Using a chemiluminescent system, chemical cross-linking of bFGF-DIG with FGF receptors was analyzed directly on Western blots of cell extracts with anti-digoxigenin antibodies. The labeling pattern was identical to that reported with iodinated bFGF, showing that bFGF-DIG bound to the same receptors. The time course of intracellular degradation of internalized bFGF-DIG was also followed by immunodetection on Western blots: the low speed of the catabolic process and the size of the degradation products were comparable to those previously described with iodinated bFGF. In parallel, bFGF-DIG was readily detected by immunofluorescence in cultured cells, and was shown to be an interesting probe to determine bFGF endocytosis pathways by electron microscopy. bFGF-DIG appeared as a multifunctional nonradioactive probe suitable for combined biochemical and cytological studies of bFGF.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Aorta, Thoracic
  • Blotting, Western / methods
  • Cattle
  • Cell Division / drug effects
  • Cell Line
  • Cells, Cultured
  • Cricetinae
  • Digoxigenin*
  • Endocytosis
  • Endothelium, Vascular / metabolism*
  • Enzyme-Linked Immunosorbent Assay / methods
  • Fibroblast Growth Factor 2 / analysis*
  • Fibroblast Growth Factor 2 / metabolism
  • Fibroblast Growth Factor 2 / pharmacology
  • Fluorescent Antibody Technique
  • Humans
  • Indicators and Reagents
  • Kinetics
  • Microscopy, Electron / methods
  • Receptors, Fibroblast Growth Factor / isolation & purification
  • Receptors, Fibroblast Growth Factor / metabolism*
  • Recombinant Proteins / analysis
  • Recombinant Proteins / metabolism
  • Recombinant Proteins / pharmacology
  • Sensitivity and Specificity

Substances

  • Indicators and Reagents
  • Receptors, Fibroblast Growth Factor
  • Recombinant Proteins
  • Fibroblast Growth Factor 2
  • Digoxigenin