Preliminary electron crystallographic analysis of ice-embedded tropomyosin crystals

J Struct Biol. 1993 Jan-Feb;110(1):67-74. doi: 10.1006/jsbi.1993.1005.

Abstract

Electron images and diffraction patterns of ice-embedded tropomyosin crystalline sheets have been recorded at 100 and 400 kV. Optical diffractograms from the images indicated an elongated, centered unit cell with a = 799.2 +/- 10.6 A, b = 55.1 +/- 3.5 A. Evaluation of the phases in the computed Fourier transforms up to 7 A resolution revealed the presence of symmetry axes consistent with two-dimensional space group cmm. Electron diffraction patterns show diffuse arcs and discrete sampling at a resolution of 5.1 A, arising from the alpha-helical coiled-coil features of the molecule. These results demonstrate that tropomyosin thin sheets are highly ordered and suggest that retrieval of its high-resolution three-dimensional structure may be feasible by electron crystallography.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Animals
  • Crystallography
  • Electrons
  • Ice
  • In Vitro Techniques
  • Microscopy, Electron / methods
  • Swine
  • Tropomyosin / ultrastructure*

Substances

  • Ice
  • Tropomyosin