An analysis of the conformational changes that accompany the activation and inhibition of gelatinase A

FEBS Lett. 1996 Feb 12;380(1-2):53-7. doi: 10.1016/0014-5793(96)00005-1.

Abstract

The latent precursors of the matrix metalloproteinases (MMPs) are converted by (4-aminophenylmercuric)acetate to active forms that lose their propeptide as a result of autolysis. C.D. and an active site mutant of progelatinase A (MMP2) were used to demonstrate that, although propeptide removal is accompanied by a decrease in the enzyme's beta-sheet content, the initial activation is achieved with only minor modifications to the conformation. Mixing activated gelatinase A with the natural inhibitor, TIMP-1, resulted in conformational changes that were absent when a synthetic inhibitor was used. The relevance of these results to MMP activation and inhibition is discussed.

MeSH terms

  • Amino Acid Sequence
  • Circular Dichroism
  • Enzyme Activation / drug effects
  • Gelatinases / antagonists & inhibitors*
  • Gelatinases / chemistry*
  • Gelatinases / metabolism
  • Glycoproteins / pharmacology
  • Humans
  • Matrix Metalloproteinase 2
  • Metalloendopeptidases / antagonists & inhibitors*
  • Metalloendopeptidases / chemistry*
  • Metalloendopeptidases / metabolism
  • Molecular Sequence Data
  • Molecular Weight
  • Mutation
  • Phenylmercuric Acetate / analogs & derivatives
  • Phenylmercuric Acetate / pharmacology
  • Protease Inhibitors / pharmacology
  • Protein Conformation
  • Protein Precursors / chemistry
  • Tissue Inhibitor of Metalloproteinases

Substances

  • Glycoproteins
  • Protease Inhibitors
  • Protein Precursors
  • Tissue Inhibitor of Metalloproteinases
  • 4-aminophenylmercuriacetate
  • Gelatinases
  • Metalloendopeptidases
  • Matrix Metalloproteinase 2
  • Phenylmercuric Acetate