Synthesis and characterization of bivalent peptide ligands targeted to G-protein-coupled receptors

Chem Biol. 1996 Jul;3(7):537-42. doi: 10.1016/s1074-5521(96)90144-1.

Abstract

Background: Through the effects of avidity, multivalency can increase the apparent affinity of a ligand for its binding site. Low molecular weight, high affinity, multivalent ligands theoretically could be used to deliver a variety of agents to specific cell subtypes. In order to target specific G-protein-coupled receptors, a series of monospecific peptide dimers were synthesized that are designed to bind to two adjacent receptor sites.

Results: Three dimers, consisting of a ligand region, a short, flexible, uncharged spacer, a longer, polylysine spacer and a single cysteine residue to permit dimerization, and the corresponding monomers were synthesized by solid-phase peptide synthesis. The ligand domain was either alpha-melanocyte stimulating hormone (alpha-MSH), an alpha-MSH receptor antagonist (alpha-MSH-ANT), or bombesin. These ligands were characterized in a functional melanocyte dispersion assay. In wild-type melanophores, the alpha-MSH dimer stimulated dispersion with an EC50 approximately seven-fold lower than that of the corresponding monomer. Similarly, in cells transfected with bombesin receptor cDNA, the bombesin dimer was approximately five-fold more potent than the monomer. The alpha-MSH-ANT monomer specifically inhibited alpha-MSH-mediated dispersion with no significant agonist activity, but the dimer acted predominantly as an agonist.

Conclusions: Peptide dimers can be synthesized easily and have enhanced functional activity; monospecific dimers have greater avidity and bispecific dimers are likely to have greater selectivity. They may therefore have practical potential as specific cell-targeting agents.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Binding Sites
  • Bombesin / chemistry
  • Bombesin / metabolism
  • Dimerization
  • GTP-Binding Proteins / metabolism*
  • In Vitro Techniques
  • Ligands
  • Melanocytes / metabolism
  • Molecular Sequence Data
  • Molecular Structure
  • Peptides / chemical synthesis
  • Peptides / chemistry*
  • Peptides / metabolism*
  • Receptors, Bombesin / genetics
  • Receptors, Bombesin / metabolism
  • Receptors, Cell Surface / metabolism*
  • Transfection
  • Xenopus laevis
  • alpha-MSH / antagonists & inhibitors
  • alpha-MSH / metabolism

Substances

  • Ligands
  • Peptides
  • Receptors, Bombesin
  • Receptors, Cell Surface
  • alpha-MSH
  • GTP-Binding Proteins
  • Bombesin