Detection of DNA bending in a DNA-PAP1 protein complex by fluorescence resonance energy transfer

Biochem Biophys Res Commun. 1997 Feb 24;231(3):553-6. doi: 10.1006/bbrc.1997.6138.

Abstract

The structure of DNA in a DNA-protein complex was studied by means of fluorescence resonance energy transfer (FRET) method. Oligonucleotide phosphorothioates were labeled with fluorescein and eosin to obtain a donor- and acceptor-labeled DNA. The formation of a complex of the DNA with PAP1(70), which is a DNA binding site fragment derived from transcription regulatory protein, PAP1, of fission yeast, was confirmed by gel retardation analysis and fluorescence measurements. FRET of the donor- and acceptor-labeled DNA with and without PAP1(70) indicated that the DNA in the complex was bent about 26 degrees toward the protein-binding surface.

MeSH terms

  • Basic-Leucine Zipper Transcription Factors
  • Binding Sites
  • DNA-Binding Proteins / chemistry*
  • DNA-Binding Proteins / metabolism
  • Deoxyribonucleoproteins / chemistry*
  • Energy Transfer
  • Fungal Proteins / chemistry
  • Nucleic Acid Conformation*
  • Oligodeoxyribonucleotides / chemistry
  • Pancreatitis-Associated Proteins
  • Schizosaccharomyces
  • Schizosaccharomyces pombe Proteins
  • Spectrometry, Fluorescence
  • Transcription Factors / chemistry*

Substances

  • Basic-Leucine Zipper Transcription Factors
  • DNA-Binding Proteins
  • Deoxyribonucleoproteins
  • Fungal Proteins
  • Oligodeoxyribonucleotides
  • Pancreatitis-Associated Proteins
  • Pap1 protein, S pombe
  • REG3A protein, human
  • Schizosaccharomyces pombe Proteins
  • Transcription Factors