Decreased substrate affinity upon alteration of the substrate-docking region in cytochrome P450(BM-3)

FEBS Lett. 1997 Sep 8;414(2):213-8. doi: 10.1016/s0014-5793(97)00999-x.

Abstract

A mutation at the surface of the substrate access channel which dramatically decreases the affinity for some fatty acids in P450(BM-3) was discovered by random mutagenesis. The mutation introduced, proline-25 to glutamine, is in close proximity to the arginine-47 residue thought to be responsible for the initial docking of fatty acid substrates. The P25Q mutant displays an affinity for palmitate which is approximately 100-fold weaker than the wild-type enzyme. In addition to its altered substrate affinity, P25Q also exhibits altered hydroxylation specificity and carbon monoxide recombination kinetics in the substrate-free form.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Arginine
  • Bacterial Proteins*
  • Binding Sites
  • Cloning, Molecular
  • Cytochrome P-450 Enzyme System / chemistry*
  • Cytochrome P-450 Enzyme System / metabolism*
  • Escherichia coli
  • Glutamine
  • Kinetics
  • Lauric Acids / metabolism
  • Mixed Function Oxygenases / chemistry*
  • Mixed Function Oxygenases / metabolism*
  • Models, Structural
  • Mutagenesis, Site-Directed
  • Myristic Acid
  • Myristic Acids / metabolism
  • NADPH-Ferrihemoprotein Reductase
  • Palmitic Acid / metabolism
  • Point Mutation
  • Proline
  • Protein Structure, Secondary*
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / metabolism
  • Substrate Specificity
  • Thermodynamics

Substances

  • Bacterial Proteins
  • Lauric Acids
  • Myristic Acids
  • Recombinant Proteins
  • Myristic Acid
  • Glutamine
  • lauric acid
  • Palmitic Acid
  • Cytochrome P-450 Enzyme System
  • Arginine
  • Proline
  • Mixed Function Oxygenases
  • NADPH-Ferrihemoprotein Reductase
  • flavocytochrome P450 BM3 monoxygenases