A radioreceptor assay for mass measurement of inositol (1,4,5)-trisphosphate using saponin-permeabilized outdated human platelets

Anal Biochem. 1998 Feb 1;256(1):117-21. doi: 10.1006/abio.1997.2488.

Abstract

The binding of inositol 1,4,5-trisphosphate [Ins(1,4,5)P3] to saponin-permeabilized blood-bank-outdated human platelets, 6 days old, has been characterized (Kd = 3.8 nM; Bmax = 1.7 pmol/mg protein) and used to develop a novel radioreceptor assay which allows the measurement of the Ins(1,4,5)P3 content in resting or agonist-stimulated cells. This assay is as sensitive (0.25 pmol in a 0.25 ml volume), specific, and reproducible as previously proposed methods. In addition, obtaining large batches of the Ins(1,4,5)P3 binding protein by treating outdated platelets with saponin is simple and quick and uses otherwise discarded material. Moreover, the assay is considerably cheaper than commercially available kits. Using this method we confirmed that thrombin evokes a rapid, transient, and dose-dependent increase in the platelet concentration of Ins(1,4,5)P3.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Blood Platelets / drug effects
  • Blood Platelets / metabolism*
  • Humans
  • In Vitro Techniques
  • Inositol 1,4,5-Trisphosphate / analysis*
  • Inositol 1,4,5-Trisphosphate / metabolism
  • Kinetics
  • Permeability
  • Radioligand Assay / methods*
  • Radioligand Assay / statistics & numerical data
  • Reproducibility of Results
  • Saponins
  • Sensitivity and Specificity
  • Thrombin / pharmacology

Substances

  • Saponins
  • Inositol 1,4,5-Trisphosphate
  • Thrombin