Purification and characterisation of an intracellular X-prolyl-dipeptidyl aminopeptidase from Streptococcus thermophilus ACA-DC 4

J Biotechnol. 1997 Jan 3;59(3):203-11. doi: 10.1016/s0168-1656(97)00157-0.

Abstract

An intracellular X-prolyl-dipeptidyl aminopeptidase from Streptococcus thermophilus ACA-DC 4, isolated from traditional Greek yoghurt, was purified by anion exchange and gel filtration chromatography. A single band of molecular weight of about 80,000 appeared in SDS-PAGE; by gel filtration it was shown that the native enzyme was dimeric. The peptidase showed optimum activity on glycyl-prolyl 4-nitroanilide at pH 7.0 and at 50 degrees C, with K(m) = 3.1 mM and Vmax = 3500 U mg-1; over 50 degrees C the enzyme activity declined rapidly. It was inactivated by PMSF; sulfhydryl group reagents and metal chelators had little effect on enzyme activity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Anilides / metabolism
  • Caseins / metabolism
  • Dimerization
  • Dipeptidyl-Peptidases and Tripeptidyl-Peptidases / chemistry*
  • Enzyme Inhibitors / pharmacology
  • Enzyme Stability
  • Hydrogen-Ion Concentration
  • Kinetics
  • Molecular Weight
  • Proline / metabolism
  • Protein Conformation
  • Streptococcus / enzymology*
  • Substrate Specificity
  • Temperature
  • Tosyl Compounds / pharmacology
  • Yogurt / microbiology*

Substances

  • Anilides
  • Caseins
  • Enzyme Inhibitors
  • Tosyl Compounds
  • 4-toluenesulfonyl fluoride
  • Proline
  • Dipeptidyl-Peptidases and Tripeptidyl-Peptidases