Large-scale preparation of the delta10 form of staphylokinase by in vitro processing of recombinant staphylokinase with purified human plasminogen

Appl Biochem Biotechnol. 1998 Mar;69(3):147-56. doi: 10.1007/BF02788810.

Abstract

The authors have developed a rapid and convenient method for purification of a low molecular weight form (delta 10) of the bacterial plasminogen activator, staphylokinase. Recombinant staphylokinase is expressed in Escherichia coli, with an amino terminal extension that facilitated purification by immobilized metal-affinity chromatography. Purified staphylokinase is treated with human plasminogen, and the resulting truncated form is purified using a combination of immobilized metal affinity chromatography and hydrophobic interaction chromatography. Purified protein is characterized by amino terminal sequencing and in vitro plasminogen activation assay.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Escherichia coli / genetics
  • Humans
  • In Vitro Techniques
  • Metalloendopeptidases / chemistry
  • Metalloendopeptidases / genetics
  • Metalloendopeptidases / isolation & purification*
  • Molecular Weight
  • Plasminogen* / isolation & purification
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Staphylococcus aureus / enzymology
  • Staphylococcus aureus / genetics

Substances

  • Recombinant Proteins
  • Plasminogen
  • Metalloendopeptidases
  • auR protein, Staphylococcus aureus