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Attribution of the discrepancy between ELISA and LC-MS/MS assay results of a PEGylated scaffold protein in post-dose monkey plasma samples due to the presence of anti-drug antibodies.
Wang SJ, Wu ST, Gokemeijer J, Fura A, Krishna M, Morin P, Chen G, Price K, Wang-Iverson D, Olah T, Weiner R, Tymiak A, Jemal M. Wang SJ, et al. Among authors: jemal m. Anal Bioanal Chem. 2012 Jan;402(3):1229-39. doi: 10.1007/s00216-011-5527-9. Epub 2011 Dec 1. Anal Bioanal Chem. 2012. PMID: 22130720
A strategy for liquid chromatography/tandem mass spectrometry based quantitation of pegylated protein drugs in plasma using plasma protein precipitation with water-miscible organic solvents and subsequent trypsin digestion to generate surrogate peptides for detection.
Wu ST, Ouyang Z, Olah TV, Jemal M. Wu ST, et al. Among authors: jemal m. Rapid Commun Mass Spectrom. 2011 Jan 30;25(2):281-90. doi: 10.1002/rcm.4856. Rapid Commun Mass Spectrom. 2011. PMID: 21192023
LC-MS/MS method using unbonded silica column and aqueous/methanol mobile phase for the simultaneous quantification of a drug candidate and co-administered metformin in rat plasma.
Discenza L, D'Arienzo C, Olah T, Jemal M. Discenza L, et al. Among authors: jemal m. J Chromatogr B Analyt Technol Biomed Life Sci. 2010 Jun 1;878(19):1583-9. doi: 10.1016/j.jchromb.2010.04.018. Epub 2010 Apr 24. J Chromatogr B Analyt Technol Biomed Life Sci. 2010. PMID: 20451474
High-field asymmetric waveform ion mobility spectrometry coupled with liquid chromatography/electrospray ionization tandem mass spectrometry (LC/ESI-FAIMS-MS/MS) multi-component bioanalytical method development, performance evaluation and demonstration of the constancy of the compensation voltage with change of mobile phase composition or flow rate.
Wu ST, Xia YQ, Jemal M. Wu ST, et al. Among authors: jemal m. Rapid Commun Mass Spectrom. 2007;21(22):3667-76. doi: 10.1002/rcm.3264. Rapid Commun Mass Spectrom. 2007. PMID: 17939154
Quantification of 4-beta-hydroxycholesterol in human plasma using automated sample preparation and LC-ESI-MS/MS analysis.
Goodenough AK, Onorato JM, Ouyang Z, Chang S, Rodrigues AD, Kasichayanula S, Huang SP, Turley W, Burrell R, Bifano M, Jemal M, LaCreta F, Tymiak A, Wang-Iverson D. Goodenough AK, et al. Among authors: jemal m. Chem Res Toxicol. 2011 Sep 19;24(9):1575-85. doi: 10.1021/tx2001898. Epub 2011 Jul 21. Chem Res Toxicol. 2011. PMID: 21728364
Targeted quantitative bioanalysis in plasma using liquid chromatography/high-resolution accurate mass spectrometry: an evaluation of global selectivity as a function of mass resolving power and extraction window, with comparison of centroid and profile modes.
Xia YQ, Lau J, Olah T, Jemal M. Xia YQ, et al. Among authors: jemal m. Rapid Commun Mass Spectrom. 2011 Oct 15;25(19):2863-78. doi: 10.1002/rcm.5178. Rapid Commun Mass Spectrom. 2011. PMID: 21913265
157 results