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Tertiary Chiral Nanostructures from C-H⋅⋅⋅F Directed Assembly of Chiroptical Superatoms.
Shen H, Xu Z, Wang L, Han YZ, Liu X, Malola S, Teo BK, Häkkinen H, Zheng N. Shen H, et al. Angew Chem Int Ed Engl. 2021 Oct 4;60(41):22411-22416. doi: 10.1002/anie.202108141. Epub 2021 Sep 1. Angew Chem Int Ed Engl. 2021. PMID: 34347339
A novel synthetic strategy, using chiral reducing agent, R and S-BINAPCuBH(4) (BINAP is 2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl), is developed to access to atomically precise, intrinsically chiral [Au(7) Ag(6) Cu(2) (R- or S-BINAP)(3) (SCH(2) Ph)(6) ]SbF(6) nano …
A novel synthetic strategy, using chiral reducing agent, R and S-BINAPCuBH(4) (BINAP is 2,2'-Bis(diphenylphosphino)-1,1'-binaphthyl), …
Organocatalytic Asymmetric Synthesis of an Advanced Intermediate of (+)-Sarain A.
Hu XN, Wu DP, Xu YP, Huang PQ. Hu XN, et al. Chemistry. 2021 Jan 7;27(2):609-613. doi: 10.1002/chem.202004261. Epub 2020 Dec 1. Chemistry. 2021. PMID: 33044771
This approach featured the employment of an organocatalytic asymmetric Michael addition reaction and a nitrogen-to-carbon chirality transfer to forge three chiral centers, as well as a catalytic hydrosilylation for the chemoselective reduction of a key lactam intermediate. …
This approach featured the employment of an organocatalytic asymmetric Michael addition reaction and a nitrogen-to-carbon chirality transfer …
Alkynyl-Protected Chiral Bimetallic Ag22 Cu7 Superatom with Multiple Chirality Origins.
Deng G, Lee K, Deng H, Malola S, Bootharaju MS, Häkkinen H, Zheng N, Hyeon T. Deng G, et al. Angew Chem Int Ed Engl. 2023 Mar 13;62(12):e202217483. doi: 10.1002/anie.202217483. Epub 2023 Jan 18. Angew Chem Int Ed Engl. 2023. PMID: 36581588
Furthermore, the circular dichroism spectra of R/S-Ag(22) Cu(7) are obtained by employing appropriate chiral molecules as optical enrichment agents. ...
Furthermore, the circular dichroism spectra of R/S-Ag(22) Cu(7) are obtained by employing appropriate chiral molecules as optical enr …
Concise Total Synthesis of (-)-Quinocarcin Enabled by Catalytic Enantioselective Reductive 1,3-Dipolar Cycloaddition of Secondary Amides.
Ji KL, He SF, Xu DD, He WX, Zheng JF, Huang PQ. Ji KL, et al. Angew Chem Int Ed Engl. 2023 Jun 19;62(25):e202302832. doi: 10.1002/anie.202302832. Epub 2023 May 8. Angew Chem Int Ed Engl. 2023. PMID: 37025034
A catalytic enantioselective reductive 1,3-dipolar cycloaddition reaction of N-heteroaryl secondary amides with reactive dipolarophiles using iridium/copper relay catalysis was developed to prepare the key chiral pyrrolidine intermediate with three stereocenters. This prot …
A catalytic enantioselective reductive 1,3-dipolar cycloaddition reaction of N-heteroaryl secondary amides with reactive dipolarophiles usin …
Kernel Homology in Gold Nanoclusters.
Zhuang S, Liao L, Yuan J, Wang C, Zhao Y, Xia N, Gan Z, Gu W, Li J, Deng H, Yang J, Wu Z. Zhuang S, et al. Angew Chem Int Ed Engl. 2018 Nov 19;57(47):15450-15454. doi: 10.1002/anie.201808997. Epub 2018 Oct 25. Angew Chem Int Ed Engl. 2018. PMID: 30290044
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