Standardization of Alternaria alternata: extraction and quantification of alt a 1 by using an mAb-based 2-site binding assay

J Allergy Clin Immunol. 1999 Jul;104(1):128-35. doi: 10.1016/s0091-6749(99)70124-7.

Abstract

Background: Alternaria alternata is recognized as an important cause of allergic disease. As with other molds, the extracts of A alternata used for diagnosis and therapy are highly heterogeneous, and there is a need for improved standardization. The major allergen Alt a 1 is well characterized and has been produced as a recombinant protein, but very few data are available on the Alt a 1 content in extracts.

Objective: An assay for the quantification of Alt a 1 was developed and used for monitoring batch-to-batch consistency of A alternata extracts, and the correlation between skin prick test responses and Alt a 1 concentrations was studied.

Methods: A 2-site binding assay based on an Alt a 1-specific mAb was developed and used for the quantification of Alt a 1 in allergen extracts. Quantitative skin prick tests were performed on 16 A alternata-sensitive patients and correlated with the Alt a 1 concentration.

Results: The Alt a 1-specific mAb was found to be suitable for affinity purification, as well as for a 2-site binding quantification assay. In allergen extracts the Alt a 1 content was estimated as 2% to 4.7% of total protein. Quantitative skin prick tests showed an Alt a 1 concentration-dependent response.

Conclusion: Quantification of Alt a 1 in A alternata extracts reflects their batch-to-batch consistency. Skin prick test responses to a standardized A alternata extract correlate with the Alt a 1 contents. An extract containing 3.7 microgram/mL Alt a 1 caused a response equal to that of a 1% histamine dihydrochloride solution.

MeSH terms

  • Allergens / immunology
  • Alternaria*
  • Amino Acid Sequence
  • Animals
  • Antibodies, Monoclonal / metabolism
  • Antigens, Plant
  • Binding Sites, Antibody
  • Fungal Proteins / immunology
  • Fungal Proteins / isolation & purification
  • Mice
  • Mice, Inbred BALB C
  • Plant Extracts / standards
  • Rabbits
  • Skin Tests

Substances

  • ALTA1 protein, Alternaria alternata
  • Allergens
  • Antibodies, Monoclonal
  • Antigens, Plant
  • Fungal Proteins
  • Plant Extracts