Ab initio studies of some amino acid residue complexes with 4-mercaptopyridine as a model for thymitaq (AG337), an inhibitor of thymidylate synthase

Cancer Invest. 1999;17(6):396-401. doi: 10.3109/07357909909021431.

Abstract

The complex formed by isopentane, as a model for the isoleucine residue present in the wild-type thymidylate synthase, with 4-mercaptopyridine as a fragment of the thymidylate synthase inhibitor Thymitaq (AG337) is investigated with ab initio quantum chemical calculations at Hartree-Fock and MP2 levels, using the 3-21G* basis set. The binding energy is compared with the binding energies of 4-mercaptopyridine with amino acid residues found in mutant thymidylate synthase enzymes. As compared with isoleucine, alanine and glycine do not show binding, in agreement with enzyme-inhibition results.

MeSH terms

  • Acetamides / chemistry
  • Acetamides / metabolism
  • Amino Acids / chemistry
  • Amino Acids / metabolism*
  • Benzene / chemistry
  • Benzene / metabolism
  • Binding Sites
  • Electrons
  • Hydrogen / chemistry
  • Hydrogen / metabolism
  • Ions
  • Methane / chemistry
  • Methane / metabolism
  • Models, Chemical*
  • Pentanes / chemistry
  • Pentanes / metabolism
  • Pyridines / chemistry
  • Pyridines / metabolism*
  • Quinazolines / chemistry*
  • Quinazolines / metabolism
  • Quinazolines / pharmacology
  • Thermodynamics
  • Thymidylate Synthase / antagonists & inhibitors*
  • Thymidylate Synthase / chemistry
  • Thymidylate Synthase / genetics
  • Thymidylate Synthase / metabolism

Substances

  • Acetamides
  • Amino Acids
  • Ions
  • Pentanes
  • Pyridines
  • Quinazolines
  • 4-thiopyridine
  • Hydrogen
  • acetamide
  • Thymidylate Synthase
  • Benzene
  • nolatrexed
  • Methane
  • isopentane