Purification and properties of genetic expressing product of thermostable protease from Bacillus stearothermophilus HY-69

Chin J Biotechnol. 1999;15(1):15-21.

Abstract

The thermostable metal protease gene from Bacillus stearothermophilus HY-69 had been cloned and expressed in Bacillus subtilis MI113. The genetic expressing product of the enzyme was purified by CM-cellulose chromatography. The product shows homogeneity on PAGE. Its molecular weight is 27,000 +/- 1000 by SDS-PAGE and Sephadex G100 filtration, respectively. The alpha-helix content of the protease is estimated to be about 66%, the beta-turn about 28%, the random coil about 6%, but not beta-sheet, calculated from the circular dichroism data. The optimal temperature of the enzyme was 70 degrees C. When the enzyme was denatured in 3 mol/L of Gdn--HCl in phosphate buffer pH6.0 for 20 min, it remained about 40% of original activity. It shows that it is rather resistant to heat and Gdn-HCl denaturation. Its conformational variety coursed by Gdn-HCl was investigated by the far UV circular dichroism and fluorescence spectra. The results show that the enzyme has more compact conformation and internal hydrophobility.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acids / analysis
  • Bacillus subtilis / enzymology
  • Bacillus subtilis / genetics
  • Circular Dichroism
  • Cloning, Molecular
  • Electrophoresis, Polyacrylamide Gel
  • Endopeptidases / chemistry*
  • Endopeptidases / genetics
  • Endopeptidases / isolation & purification
  • Enzyme Stability
  • Geobacillus stearothermophilus / chemistry*
  • Heating
  • Molecular Weight
  • Protein Denaturation
  • Spectrometry, Fluorescence

Substances

  • Amino Acids
  • Endopeptidases