Annexins V and XII insert into bilayers at mildly acidic pH and form ion channels

Biochemistry. 2000 Mar 21;39(11):3015-22. doi: 10.1021/bi9922401.

Abstract

The functional hallmark of annexins is the ability to bind to the surface of phospholipid membranes in a reversible, Ca(2+)-dependent manner. We now report that human annexin V and hydra annexin XII reversibly bound to phospholipid vesicles in the absence of Ca(2+) at low pH; half-maximal vesicle association occurred at pH 5.3 and 5. 8, respectively. The following biochemical data support the hypothesis that these annexins insert into bilayers at mildly acidic pH. First, a photoactivatable reagent (3-trifluoromethyl)-3-(m-[(125)I]iodophenyl)diazirine) which selectively labels proteins exposed to the hydrophobic domain of bilayers reacted with these annexins at pH 5.0 and below but not at neutral pH. Second, in a Triton X-114 partitioning assay, annexins V and XII act as integral membrane proteins at low pH and as hydrophilic proteins at neutral pH; in the presence of phospholipids half-maximal partitioning into detergent occurred at pH approximately 5.0. Finally, annexin V or XII formed single channels in phospholipid bilayers at low pH but not at neutral pH. A model is discussed in which the concentrations of H(+) and Ca(2+) regulate the reversible conversion of three forms of annexins-soluble, peripheral membrane, and transmembrane.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Alkanesulfonic Acids / chemistry
  • Animals
  • Annexin A5 / chemistry*
  • Annexins / chemistry
  • Azirines / chemistry
  • Buffers
  • Humans
  • Hydra
  • Hydrogen-Ion Concentration
  • Iodine Radioisotopes
  • Ion Channels / chemistry*
  • Lipid Bilayers / chemistry*
  • Morpholines / chemistry
  • Octoxynol
  • Phospholipids / chemistry
  • Photoaffinity Labels / chemistry
  • Polyethylene Glycols / chemistry
  • Sodium Acetate / chemistry
  • Spin Labels
  • Tromethamine / chemistry

Substances

  • Alkanesulfonic Acids
  • Annexin A5
  • Annexins
  • Azirines
  • Buffers
  • Iodine Radioisotopes
  • Ion Channels
  • Lipid Bilayers
  • Morpholines
  • Phospholipids
  • Photoaffinity Labels
  • Spin Labels
  • Tromethamine
  • 2-(N-morpholino)ethanesulfonic acid
  • Polyethylene Glycols
  • Sodium Acetate
  • 3-(trifluoromethyl)-3-(3-iodophenyl)diazirine
  • Octoxynol
  • Nonidet P-40