Synthesis and characterization of a fluorescent substrate for the N-arachidonoylethanolamine (anandamide) transmembrane carrier

J Pharmacol Exp Ther. 2000 Apr;293(1):289-95.

Abstract

N-Arachidonoylethanolamine (AEA) is a proposed endogenous ligand of the central cannabinoid receptor (CB1). Previous studies indicate that AEA is translocated across membranes via a process that has the characteristics of carrier-mediated facilitated diffusion. To date, studies of this mechanism have relied on [(3)H]AEA as a substrate for the carrier. We have synthesized an analog of AEA, SKM 4-45-1, that is nonfluorescent in the extracellular environment. When SKM 4-45-1 is exposed to intracellular esterases, it is de-esterified and becomes fluorescent. We have carried out studies to demonstrate that SKM 4-45-1 accumulation in cells occurs via the AEA carrier. SKM 4-45-1 is accumulated by both cerebellar granule cells and C6 glioma cells. Uptake of SKM 4-45-1 into C6 glioma is inhibited by AEA (IC(50)=53.8 +/- 1.8 microM), arachidonoyl-3-aminopyridine amide (IC(50)=10.1 +/- 1.4 microM), and arachidonoyl-4-hydroxyanilineamide (IC(50)=6.1 +/- 1.3 microM), all of which also inhibit [(3)H]AEA accumulation. Conversely, [(3)H]AEA accumulation by cerebellar granule cells is inhibited by SKM 4-45-1 with an IC(50) of 7.8 +/- 1. 3 microM. SKM 4-45-1 is neither a substrate nor inhibitor of fatty acid amide hydrolase, an enzyme that catabolizes AEA. SKM 4-45-1 does not bind the CB1 cannabinoid receptor at concentrations <10 microM. In summary, the cellular accumulation of SKM 4-45-1 occurs via the same pathway as AEA uptake and provides an alternative substrate for the study of this important cellular process.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amidohydrolases / metabolism
  • Animals
  • Arachidonic Acids / metabolism*
  • Brain Neoplasms / metabolism
  • Cannabinoids / metabolism
  • Carrier Proteins / metabolism
  • Cell Membrane / metabolism
  • Cerebellum / cytology
  • Cerebellum / drug effects
  • Cerebellum / metabolism
  • Cyclohexanols / metabolism
  • Endocannabinoids
  • Esterases / chemistry
  • Fluorescent Dyes / chemical synthesis
  • Fluorescent Dyes / metabolism*
  • Glioma / metabolism
  • Humans
  • Lactones / chemical synthesis
  • Lactones / metabolism*
  • Microscopy, Fluorescence
  • Polyunsaturated Alkamides
  • Rats
  • Rats, Sprague-Dawley
  • Tumor Cells, Cultured

Substances

  • Arachidonic Acids
  • Cannabinoids
  • Carrier Proteins
  • Cyclohexanols
  • Endocannabinoids
  • Fluorescent Dyes
  • Lactones
  • Polyunsaturated Alkamides
  • SKM 4-45-1
  • 3-(2-hydroxy-4-(1,1-dimethylheptyl)phenyl)-4-(3-hydroxypropyl)cyclohexanol
  • Esterases
  • Amidohydrolases
  • fatty-acid amide hydrolase
  • anandamide