Rhodopsin kinase: expression in mammalian cells and a two-step purification

Proc Natl Acad Sci U S A. 2000 Mar 28;97(7):3004-9. doi: 10.1073/pnas.97.7.3004.

Abstract

A suitable system for expression of the rhodopsin kinase (RK) gene and its mutants is needed for structure-function studies of RK. Previously, investigation of the baculovirus system showed satisfactory production of RK, but posttranslational isoprenylation was deficient. We now report on a comparative study of expression of the RK gene in yeast (Pichia pastoris), COS-1 cells and in an HEK293 stable cell line. Expression in COS-1 cells, by using pCMV5 vector, is the most satisfactory. A two-step procedure for purification of the expressed enzyme with an N-terminal histidine tag has been developed. The purified enzyme has correct posttranslational modifications and shows a somewhat broader pH vs. catalytic activity profile than the wild-type enzyme.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Adenosine Triphosphate / metabolism
  • Animals
  • COS Cells
  • Cattle
  • Cell Line
  • Chromatography, Liquid
  • Cloning, Molecular
  • Electrophoresis, Polyacrylamide Gel
  • Eye Proteins*
  • G-Protein-Coupled Receptor Kinase 1
  • Humans
  • Hydrogen-Ion Concentration
  • Protein Kinases / genetics*
  • Protein Kinases / isolation & purification
  • Protein Kinases / metabolism
  • Protein Prenylation
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Recombinant Proteins / metabolism
  • Retina / enzymology

Substances

  • Eye Proteins
  • Recombinant Proteins
  • Adenosine Triphosphate
  • Protein Kinases
  • G-Protein-Coupled Receptor Kinase 1
  • GRK1 protein, human