Purification and characterization of a novel UV lesion-specific DNA glycosylase/AP lyase from Bacillus sphaericus

Mutat Res. 2000 May 31;459(4):307-16. doi: 10.1016/s0921-8777(00)00009-4.

Abstract

The purification and characterization of a pyrimidine dimer-specific glycosylase/AP lyase from Bacillus sphaericus (Bsp-pdg) are reported. Bsp-pdg is highly specific for DNA containing the cis-syn cyclobutane pyrimidine dimer, displaying no detectable activity on oligonucleotides with trans-syn I, trans-syn II, (6-4), or Dewar photoproducts. Like other glycosylase/AP lyases that sequentially cleave the N--glycosyl bond of the 5' pyrimidine of a cyclobutane pyrimidine dimer, and the phosphodiester backbone, this enzyme appears to utilize a primary amine as the attacking nucleophile. The formation of a covalent enzyme-DNA imino intermediate is evidenced by the ability to trap this protein-DNA complex by reduction with sodium borohydride. Also consistent with its AP lyase activity, Bsp-pdg was shown to incise an AP site-containing oligonucleotide, yielding beta- and delta-elimination products. N-terminal amino acid sequence analysis of this 26 kDa protein revealed little amino acid homology to any previously reported protein. This is the first report of a glycosylase/AP lyase enzyme from Bacillus sphaericus that is specific for cis-syn pyrimidine dimers.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Bacillus / enzymology*
  • Bacillus / genetics
  • Bacillus / radiation effects
  • Base Sequence
  • Carbon-Oxygen Lyases / genetics
  • Carbon-Oxygen Lyases / isolation & purification*
  • Carbon-Oxygen Lyases / metabolism
  • DNA Damage
  • DNA Glycosylases
  • DNA Repair
  • DNA, Bacterial / genetics
  • DNA, Bacterial / metabolism
  • DNA, Bacterial / radiation effects
  • DNA-(Apurinic or Apyrimidinic Site) Lyase
  • Deoxyribonuclease IV (Phage T4-Induced)
  • Molecular Sequence Data
  • N-Glycosyl Hydrolases / genetics
  • N-Glycosyl Hydrolases / isolation & purification*
  • N-Glycosyl Hydrolases / metabolism
  • Pyrimidine Dimers / metabolism
  • Pyrimidine Dimers / radiation effects
  • Sequence Homology, Amino Acid
  • Substrate Specificity
  • Ultraviolet Rays

Substances

  • DNA, Bacterial
  • Pyrimidine Dimers
  • Deoxyribonuclease IV (Phage T4-Induced)
  • DNA Glycosylases
  • N-Glycosyl Hydrolases
  • Carbon-Oxygen Lyases
  • DNA-(Apurinic or Apyrimidinic Site) Lyase