Purification and characterization of polygalacturonase from banana fruit

Phytochemistry. 2000 May;54(2):147-52. doi: 10.1016/s0031-9422(00)00061-3.

Abstract

Polygalacturonase isoenzyme 3 (PG-3) was purified to homogeneity with a specific activity of 0.7 mu katal mg-1 protein from banana fruit pulp. The purified enzyme was a glycoprotein with ca. 8% carbohydrate. The molecular weight of the native enzyme was found to be 90 +/- 10 kDa with a subunit molecular weight of 29 +/- 2 kDa. The enzyme exhibited optimum activity at pH 4.3 and temperature 40 degrees C with activation energy 35.4 kJ mol-1. A unique property of the enzyme was the requirement of -SH groups for the enzyme activity. The enzyme was inhibited by p-CMB and activated by 2-ME and DTT. The inhibition of p-CMB could be reversed by DTT. The enzyme contained eight free -SH groups. The Km of the enzyme was 0.15% for polygalacturonic acid.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Carbohydrates / analysis
  • Electrophoresis, Polyacrylamide Gel
  • Molecular Weight
  • Polygalacturonase / chemistry
  • Polygalacturonase / isolation & purification*
  • Polygalacturonase / metabolism
  • Sulfhydryl Compounds / metabolism
  • Temperature
  • Zingiberales / enzymology*

Substances

  • Carbohydrates
  • Sulfhydryl Compounds
  • Polygalacturonase