6-hydroxy derivative as new desfluoroquinolone (DFQ): synthesis and DNA-binding study

Nucleosides Nucleotides Nucleic Acids. 2000 Aug;19(8):1327-36. doi: 10.1080/15257770008033055.

Abstract

A new 6-desfluoroquinolone derivative, characterized by the presence of a 6-hydroxyl group instead of the usual fluorine atom at the C-6 position, was synthesized with the aim to better understand the mechanistic role of the C-6 substituent in the quinolone/DNA/DNA-gyrase interaction. The antibacterial activity unambiguously shows that the hydroxyl group is a good substitute for the C-6 fluorine atom, especially against Gram-positive bacteria. On the contrary, it is a very weak inhibitor of the target DNA gyrase, displaying the highest IC50 value observed for all the C-6 substituted analogues. This behaviour could be explained on the basis of its DNA binding properties.

MeSH terms

  • Anti-Infective Agents / chemical synthesis*
  • Anti-Infective Agents / chemistry
  • Anti-Infective Agents / metabolism
  • Anti-Infective Agents / pharmacology
  • DNA, Bacterial / metabolism
  • DNA, Single-Stranded / metabolism
  • Enzyme Inhibitors / chemical synthesis*
  • Enzyme Inhibitors / metabolism
  • Enzyme Inhibitors / pharmacology
  • Fluorine / chemistry
  • Gram-Negative Bacteria / drug effects
  • Gram-Positive Bacteria / drug effects
  • Magnesium / metabolism
  • Microbial Sensitivity Tests
  • Molecular Structure
  • Quinolones / chemical synthesis*
  • Quinolones / chemistry
  • Quinolones / metabolism
  • Quinolones / pharmacology
  • Structure-Activity Relationship
  • Tetrahydroisoquinolines*
  • Topoisomerase II Inhibitors*

Substances

  • 1-cyclopropyl-6-hydroxy-8-methyl-4-oxo-7-(1,2,3,4-tetrahydro-2-isoquinolyl)-1,4-dihydroquinoline-3-carboxylic acid
  • Anti-Infective Agents
  • DNA, Bacterial
  • DNA, Single-Stranded
  • Enzyme Inhibitors
  • Quinolones
  • Tetrahydroisoquinolines
  • Topoisomerase II Inhibitors
  • Fluorine
  • Magnesium