Structure and function analysis of urinary trypsin inhibitor (UTI): identification of binding domains and signaling property of UTI by analysis of truncated proteins

Biochim Biophys Acta. 2001 May 5;1547(1):26-36. doi: 10.1016/s0167-4838(01)00167-4.

Abstract

The binding of urinary trypsin inhibitor (UTI) to its binding sites/receptors on tumor cells inhibits cell invasion in a number of experimental systems and that UTI downregulates constitutive and phorbol ester-induced urokinase production by certain tumor cells. To determine whether the carbohydrate moieties and core protein are required for urokinase suppression, we obtained UTI derivatives that contained O-glycoside-linked N-terminal glycopeptide (UTIm1), N-glycoside-linked C-terminal tandem Kunitz domains (UTIm2), UTI lacking O-glycoside (UTIc), asialo UTI (UTIa), UTI lacking N-glycoside (UTIn), purified Kunitz domain II of UTI (HI-8), and recombinant Kunitz domain II of UTI (R-020). The IC(50) of inhibiting binding of (125)I-labeled UTI to cells was indistinguishable for UTIa, UTIn and intact UTI, whereas the IC(50) for inhibiting binding of (125)I-labeled UTI to cells was 2.5-, 25- and 29-fold greater for UTIm1, UTIm2 and UTIc than for native UTI. We next looked at the suppression of the urokinase expression by UTI derivatives. An enzyme-linked immunosorbent assay was carried out to measure secreted and cell-associated urokinase. Intact UTI, UTIa, or UTIn effectively suppressed urokinase expression, but UTIm1, UTIm2, UTIc, HI-8 and R-020 had no significant effect. These data show that UTI requires either the N-terminal extension with the O-linked carbohydrate moiety (chondroitin 4-sulfate sugar side chain; Ala1 to Lys21 residues) or the Kunitz domain I (Lys22 to Arg77 residues) of UTI to bind to cells, but the urokinase expression was inhibited only by the O-glycoside-linked core protein without the N-glycoside side chain.

MeSH terms

  • Binding Sites
  • Binding, Competitive
  • Cell Line
  • Cell Membrane / chemistry
  • Cell Membrane / metabolism*
  • Chondroitin ABC Lyase
  • Down-Regulation
  • Electrophoresis, Polyacrylamide Gel
  • Glycoproteins / chemistry
  • Glycoproteins / isolation & purification
  • Glycoproteins / metabolism*
  • Humans
  • Metalloendopeptidases
  • Neuraminidase
  • Peptides / isolation & purification
  • Peptides / pharmacology
  • Signal Transduction*
  • Trypsin Inhibitors / chemistry
  • Trypsin Inhibitors / metabolism*
  • Tumor Cells, Cultured
  • Urokinase-Type Plasminogen Activator / metabolism

Substances

  • Glycoproteins
  • Peptides
  • Trypsin Inhibitors
  • Neuraminidase
  • Urokinase-Type Plasminogen Activator
  • Metalloendopeptidases
  • Chondroitin ABC Lyase
  • urinastatin