Expression and characterization of soluble human parainfluenza virus type 1 hemagglutinin-neuraminidase glycoprotein

J Virol Methods. 2001 Oct;98(1):53-61. doi: 10.1016/s0166-0934(01)00355-x.

Abstract

Human parainfluenza virus types 1 (hPIV-1), 2, and 3 represent significant respiratory pathogens for which no antiviral treatment is currently available. To characterize the biochemical functions of the hPIV-1 hemagglutinin-neuraminidase (HN) glycoprotein, a potential target for antiviral therapy, we cloned and expressed a soluble portion of hPIV-1 HN (amino acid residues 137-575), lacking the N-terminal hydrophobic membrane anchorage region, in insect cells using the baculovirus secretion expression system. The expressed HN protein was purified through cation-exchange chromatography followed by metal affinity chromatography, using the 6xHis epitope introduced at the carboxyl terminus of the recombinant protein. N-terminal amino acid sequence analysis of purified HN indicated that the honeybee melittin secretion signal peptide was correctly removed during post-translational processing. Further characterization revealed that the purified HN protein was N-glycosylated and exhibited neuraminidase activity whose characteristics resembled those of the native HN protein of hPIV-1 virions. The establishment of this expression and purification system has allowed us to further explore the biochemical characteristics of paramyxovirus HN and to obtain material that could be suitable for X-ray crystallography studies.

MeSH terms

  • Amino Acid Sequence
  • Animals
  • Baculoviridae / genetics
  • Cell Line
  • Genetic Vectors
  • HN Protein / biosynthesis*
  • HN Protein / chemistry
  • HN Protein / genetics
  • Humans
  • Hydrogen-Ion Concentration
  • Insecta
  • Molecular Sequence Data
  • Neuraminidase / metabolism
  • Nickel
  • Parainfluenza Virus 1, Human / metabolism*
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / genetics
  • Sodium Chloride

Substances

  • HN Protein
  • Recombinant Proteins
  • Sodium Chloride
  • Nickel
  • Neuraminidase