Purification and characterization of three galactose specific lectins from mulberry seeds (Morus sp.)

Eur J Biochem. 2001 Dec;268(23):6005-10. doi: 10.1046/j.0014-2956.2001.02470.x.

Abstract

Three lectins were extracted and purified from mulberry seeds by gel filtration of 100% ammonium sulfate saturated crude protein extract followed by ion-exchange chromatography on DEAE and CM-cellulose. The lectins were found to be homogeneous as judged by polyacrylamide disc gel electrophoresis. The molecular masses of the lectins as determined by gel filtration were 175 000 for MSL-1, 120 000 for MSL-2 and 89 500 for MSL-3. MSL-1 is dimer in nature, with the two monomers held together by disulfide bond(s), while MSL-2 and MSL-3 contain four nonidentical subunits that are held together by nonionic hydrophobic interactions. The lectins agglutinated rat red blood cells and this agglutination was inhibited specifically by galactose, methyl-alpha-d-galactopyranoside, methyl-beta-d-galactopyranoside, lactose and raffinose. The lectins MSL-1, MSL-2 and MSL-3 contained 5.7, 5.4 and 4.5% neutral sugars, respectively, and the sugar composition of the lectins was glucose and mannose for MSL-1 and galactose for both MSL-2 and MSL-3. The lectins exhibited strong cytotoxic effect in brine shrimp lethality bioassay.

MeSH terms

  • Animals
  • Artemia / drug effects
  • Carbohydrates / analysis
  • Chromatography, Gel
  • Chromatography, Ion Exchange
  • Dimerization
  • Female
  • Galactose / pharmacology
  • Hemagglutination / drug effects
  • In Vitro Techniques
  • Lectins / chemistry
  • Lectins / isolation & purification*
  • Lectins / pharmacology
  • Lectins / toxicity
  • Molecular Weight
  • Ovum / drug effects
  • Plant Lectins
  • Protein Subunits
  • Rats
  • Rosales / chemistry*
  • Seeds / chemistry

Substances

  • Carbohydrates
  • Lectins
  • Plant Lectins
  • Protein Subunits
  • Galactose