Purification of natural antikeratin autoantibodies from normal human serum and their effect on human keratinocytes cultured in vitro

Br J Dermatol. 2001 Nov;145(5):737-48. doi: 10.1046/j.1365-2133.2001.04469.x.

Abstract

Background: Antikeratin (AK) autoantibodies, circulating antibodies against epidermal keratins, have been detected in all normal human sera. However, direct evidence on the biological significance of AK autoantibodies is still lacking.

Objectives: To purify AK autoantibodies from human serum and to make a preliminary study of their biological effects on human keratinocytes.

Methods: We first extracted keratin polypeptides from human stratum corneum and analysed their purity using sodium dodecyl sulphate-polyacrylamide gel electrophoresis (SDS-PAGE). Next, a keratin affinity column was prepared with the extracted keratins, and AK autoantibodies were purified from pooled normal human serum. Antibodies obtained were identified with SDS-PAGE, enzyme-linked immunosorbent assay, immunoperoxidase staining, immunoelectron microscopy and Western blotting. The biological effect of AK autoantibodies on cultured human keratinocytes was studied using a DNA synthesis assay, 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide (MTT) colorimetric determination and cell cycle analysis.

Results: On average, 1.83 +/- 0.24 mg of antibodies could be purified from 10 mL of pooled human serum. High-titre IgG (about 1 : 70) and low-titre IgM (about 1 : 30) AK autoantibodies were obtained. The DNA synthesis assay and MTT colorimetric determination demonstrated that AK autoantibodies have a significant dose-dependent inhibitory effect on cultured keratinocytes. Correlation coefficients in the two experiments were - 0.583 and - 0.797, respectively. Cell cycle analysis indicated that a small dose of AK autoantibodies leads to inhibition of proliferation of cultured keratinocytes, whereas a large dose of AK autoantibodies causes a visible hypodiploid peak, suggesting apoptosis of keratinocytes.

Conclusions: The present research lays a solid foundation for further investigation into the biological significance of natural AK autoantibodies.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Adult
  • Aged
  • Autoantibodies / blood
  • Autoantibodies / isolation & purification*
  • Blotting, Western
  • Cell Cycle / immunology
  • Cells, Cultured
  • Chromatography, Affinity
  • DNA / biosynthesis
  • Dose-Response Relationship, Immunologic
  • Enzyme-Linked Immunosorbent Assay
  • Female
  • Humans
  • Immunoenzyme Techniques
  • Immunoglobulin G / blood
  • Immunoglobulin G / isolation & purification
  • Keratinocytes / immunology*
  • Keratins / immunology*
  • Male
  • Microscopy, Immunoelectron
  • Middle Aged

Substances

  • Autoantibodies
  • Immunoglobulin G
  • Keratins
  • DNA