Fortum stability in different disposable infusion devices by pyridine assay

J Pharm Biomed Anal. 2002 Mar 1;27(6):873-9. doi: 10.1016/s0731-7085(01)00588-x.

Abstract

The stability of ceftazidime in 5% dextrose injection and 0.9% sodium chloride injection when stored in a different disposable infusion device was determined. Solutions of ceftazidime 40 mg/ml were used to fill the drug administration devices. Stability was determined for both 5% dextrose injection and 0.9% sodium chloride injection solutions at 37 degrees C in four disposable infusion devices. Ceftazidime and its mean degradation product, pyridine, were simultaneously assayed in triplicate by a stability-indicating high-performance liquid chromatographic (HPLC) method. This method was simple, sensitive (limit of quantitation (LOQ), 2 ng injected for both compounds), rapid (run time was 7 min) and precise (mean recovery was 100.5+/-2.9 and 103.6+/-1.9% for pyridine and ceftazidime, respectively). The ceftazidime stability in the 5% dextrose solution was lower than in the 0.9% sodium chloride solution. When stored at 37 degrees C in a disposable infusion device, the stability of the ceftazidime is included in large hourly range, depending strongly on the manufacturer. The stability of ceftazidime exceed 19 h in none studied cases. The pyridine formed in 24 h was in the range of 100-400 mg depending on devices and infusions.

MeSH terms

  • Ceftazidime / administration & dosage*
  • Ceftazidime / analysis
  • Ceftazidime / chemistry*
  • Cephalosporins / administration & dosage*
  • Chromatography, High Pressure Liquid
  • Drug Stability
  • Infusion Pumps
  • Pyridines / analysis*

Substances

  • Cephalosporins
  • Pyridines
  • Ceftazidime
  • pyridine