Computational studies of tungsten-catalyzed endo-selective cycloisomerization of 4-pentyn-1-ol

J Am Chem Soc. 2002 Apr 17;124(15):4149-57. doi: 10.1021/ja017668d.

Abstract

Endo- and exo-cycloisomerizations of 4-pentyn-1-ol have been studied computationally with density functional theory, in conjunction with double-zeta and triple-zeta basis sets, both in the absence and in the presence of tungsten carbonyl catalyst. In the absence of the catalyst, both endo- and exo-cycloisomerizations have been calculated to have a very high activation barrier of approximately 50-55 kcal/mol and cannot take place. With tungsten pentacarbonyl catalyst, endo-cycloisomerization becomes a complex multiple-step reaction and proceeds with a rate-determining barrier of 26 kcal/mol at the C(alpha) --> C(beta) hydride migration step to form a vinylidene intermediate. The primary role of the tungsten catalyst is to stabilize the vinylidene intermediate, thus lowering the rate-determining barrier. The second important role of the tungsten catalyst in endo-cycloisomerization is to assist the OH hydride migration to C(alpha) by making it a multistep process with small activation barriers. The exo-cycloisomerization with the catalyst still has a high rate-determining barrier of 47 kcal/mol. These findings clearly explain the experimentally observed endo-selectivity in the cycloisomerization of 4-pentyn-1-ol derivatives and support the experimentally proposed mechanism.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Alkynes / chemistry*
  • Catalysis
  • Hydrocarbons, Cyclic / chemical synthesis*
  • Molecular Structure
  • Organometallic Compounds / chemistry*
  • Pentanols / chemistry*
  • Tungsten / chemistry*

Substances

  • 4-pentyn-1-ol
  • Alkynes
  • Hydrocarbons, Cyclic
  • Organometallic Compounds
  • Pentanols
  • Tungsten