[Determination of total scopoletin in Caulis Erycibes by RP-HPLC]

Zhongguo Zhong Yao Za Zhi. 1999 Jan;24(1):41-3, 64.
[Article in Chinese]

Abstract

Objective: To accumulate data for quality control of Caulis Erycibes.

Method: The total-scopoletin in Caulis Erycibes was determined by RP-HPLC, using CLC-ODS1 column, 0.5% glacial acetic acid in methanol-water(26:55) as mobile phase and UV detector at 310 nm.

Result: The average recovery is 99.37% and RSD 0.39%.

Conclusion: Determination data have been obtained for fourteen batches of three species, and the contents of scopoletin should be no less than 30 mg/100 g.

Publication types

  • English Abstract

MeSH terms

  • Chromatography, High Pressure Liquid / methods
  • Convolvulaceae / chemistry*
  • Drugs, Chinese Herbal / chemistry*
  • Plants, Medicinal / chemistry*
  • Quality Control
  • Scopoletin / analysis*

Substances

  • Drugs, Chinese Herbal
  • Scopoletin