Isolation of H+ -translocating ATPase in tonoplast of Tradescantia virginiana L. leaf cells

J Biotechnol. 2003 Feb 13;100(3):221-9. doi: 10.1016/s0168-1656(02)00244-4.

Abstract

The tonoplast of Tradescantia virginiana L. was prepared from leaf cells and then solubilized with deoxycholate (DOC) and n-octyl-beta-D-glucoside (n-OG). Three major polypeptides (68, 60, 16 kDa) and several other minor components were isolated. These polypeptides were reconstituted in soybean phospholipids (asolectin). The H(+) pump activity was investigated with the reconstituted system as well as with the tonoplast. In both cases, the quinacrine-fluorescence quenching was observed in the presence of ATP-Mg(2+), indicating the H(+) pumping. The H(+) pump activity was inhibited by gramicidin D, a channel-forming ionophore, and by KNO(3), an inhibitor specific to tonoplast-type (V-type) H(+)-ATPase.

MeSH terms

  • Enzyme Activation
  • Enzyme Inhibitors / chemistry
  • Hydrogen-Ion Concentration
  • Liposomes / chemistry
  • Membrane Proteins / chemistry
  • Membrane Proteins / metabolism*
  • Molecular Weight
  • Peptides / chemistry
  • Plant Leaves / chemistry
  • Plant Leaves / metabolism*
  • Plant Proteins / chemistry
  • Plant Proteins / metabolism*
  • Proton-Translocating ATPases / chemistry*
  • Proton-Translocating ATPases / isolation & purification
  • Proton-Translocating ATPases / metabolism*
  • Tradescantia / chemistry
  • Tradescantia / metabolism*

Substances

  • Enzyme Inhibitors
  • Liposomes
  • Membrane Proteins
  • Peptides
  • Plant Proteins
  • tonoplast intrinsic protein, plant
  • Proton-Translocating ATPases