Impact of N-terminal myristoylation on the Ca2+-dependent conformational transition in recoverin

J Biol Chem. 2003 Jun 20;278(25):22972-9. doi: 10.1074/jbc.M300447200. Epub 2003 Apr 9.

Abstract

Recoverin is a Ca2+-regulated signal transduction modulator found in vertebrate retina that has been shown to undergo dramatic conformational changes upon Ca2+ binding to its two functional EF-hand motifs. To elucidate the differential impact of the N-terminal myristoylation as well as occupation of the two Ca2+ binding sites on recoverin structure and function, we have investigated a non-myristoylated E85Q mutant exhibiting virtually no Ca2+ binding to EF-2. Crystal structures of the mutant protein as well as the non-myristoylated wild-type have been determined. Although the non-myristoylated E85Q mutant does not display any functional activity, its three-dimensional structure in the presence of Ca2+ resembles the myristoylated wild-type with two Ca2+ but is quite dissimilar from the myristoylated E85Q mutant. We conclude that the N-terminal myristoyl modification significantly stabilizes the conformation of the Ca2+-free protein (i.e. the T conformation) during the stepwise transition toward the fully Ca2+-occupied state. On the basis of these observations, a refined model for the role of the myristoyl group as an intrinsic allosteric modulator is proposed.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Substitution
  • Animals
  • Biomarkers, Tumor / chemistry
  • Biomarkers, Tumor / metabolism
  • Calcium / metabolism*
  • Calcium-Binding Proteins / chemistry*
  • Calcium-Binding Proteins / metabolism*
  • Cattle
  • Crystallography, X-Ray
  • Eye Proteins*
  • G-Protein-Coupled Receptor Kinase 1
  • Hippocalcin
  • Kinetics
  • Lipoproteins*
  • Models, Molecular
  • Mutagenesis, Site-Directed
  • Myristic Acid / metabolism*
  • Nerve Tissue Proteins*
  • Protein Binding
  • Protein Conformation
  • Protein Kinases / metabolism
  • Protein Structure, Secondary
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / metabolism
  • Recoverin
  • Rod Cell Outer Segment / metabolism

Substances

  • Biomarkers, Tumor
  • Calcium-Binding Proteins
  • Eye Proteins
  • Lipoproteins
  • Nerve Tissue Proteins
  • Recombinant Proteins
  • Myristic Acid
  • Recoverin
  • Hippocalcin
  • Protein Kinases
  • G-Protein-Coupled Receptor Kinase 1
  • Calcium

Associated data

  • PDB/1OMR
  • PDB/1OMV