Identification of XMAP215 as a microtubule-destabilizing factor in Xenopus egg extract by biochemical purification

J Cell Biol. 2003 Apr 28;161(2):349-58. doi: 10.1083/jcb.200211095.

Abstract

Microtubules (MTs) polymerized with GMPCPP, a slowly hydrolyzable GTP analogue, are stable in buffer but are rapidly depolymerized in Xenopus egg extracts. This depolymerization is independent of three previously identified MT destabilizers (Op18, katanin, and XKCM1/KinI). We purified the factor responsible for this novel depolymerizing activity using biochemical fractionation and a visual activity assay and identified it as XMAP215, previously identified as a prominent MT growth-promoting protein in Xenopus extracts. Consistent with the purification results, we find that XMAP215 is necessary for GMPCPP-MT destabilization in extracts and that recombinant full-length XMAP215 as well as an NH2-terminal fragment have depolymerizing activity in vitro. Stimulation of depolymerization is specific for the MT plus end. These results provide evidence for a robust MT-destabilizing activity intrinsic to this microtubule-associated protein and suggest that destabilization may be part of its essential biochemical functions. We propose that the substrate in our assay, GMPCPP-stabilized MTs, serves as a model for the pause state of MT ends and that the multiple activities of XMAP215 are unified by a mechanism of antagonizing MT pauses.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Animals
  • Biological Assay
  • Cell Extracts / chemistry*
  • Cell Extracts / pharmacology*
  • Female
  • Guanosine Triphosphate / analogs & derivatives*
  • Guanosine Triphosphate / pharmacology
  • Microtubule Proteins / biosynthesis
  • Microtubule Proteins / drug effects
  • Microtubule Proteins / genetics
  • Microtubule-Associated Proteins / isolation & purification*
  • Microtubule-Associated Proteins / pharmacology
  • Microtubules / drug effects
  • Microtubules / metabolism*
  • Models, Biological
  • Oocytes / drug effects
  • Oocytes / metabolism*
  • Protein Structure, Tertiary / physiology
  • Recombinant Fusion Proteins / pharmacology
  • Xenopus Proteins*
  • Xenopus laevis / metabolism*

Substances

  • CKAP5 protein, Xenopus
  • Cell Extracts
  • Microtubule Proteins
  • Microtubule-Associated Proteins
  • Recombinant Fusion Proteins
  • Xenopus Proteins
  • 5'-guanylylmethylenebisphosphonate
  • Guanosine Triphosphate